By Jan W. Gooch
`...In end, this e-book could be a really beneficial resource of reference for the polymer analyst operating in academia or who has to characterise and deformulate a variety of polymer products.'
Polymer checking out, 18:231-232 (1999)
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Additional info for Analysis and Deformulation of Polymeric Materials: Paints, Plastics, Adhesives, and Inks
Electrothermal vaporization using a graphite furnace provides those features. With graphite furnace atomic absorption (GFAA), the flame is replaced by an electrically heated graphite tube. A sample is introduced directly into the tube, which is then heated in a programmed series of steps to remove the solvent and major matrix components and then to atomize the remaining sample. All of the analyte is atomized, and the atoms are retained within the tube (and the light path, which passes through the tube) for an extended period.
2. Equipment The Hitachi scanning electron microscope is shown in Fig. 4. SEMs are available in different sizes, but usually in a desk-size console depending on the capabilities. Micrographs can be conveniently generated in black and white and/or color. Also, EDXRA spectrograms are usually available from the same SEM instrument. 4. Photograph of Hitachi S-4500 Scanning Electron Microscope. Reprinted with permission of Hitachi Instruments Co. lighted for the presence of elements (usually to a minimum atomic number of 5) which is very impressive in colors.
Infrared spectroscopy involves the twisting, bending, rotating, and vibrational motions of atoms in a molecule. On interaction with infrared radiation, portions of the incident radiation are absorbed at particular wavelengths. The multiplicity of vibrations occurring simultaneously produces a highly complex absorption spectrum, which is uniquely characteristic of the functional groups comprising the molecule and of the overall configuration of the atoms as well. Suggested review articles on the fundamentals of infrared spectroscopy are Bellamy (1958), Colthup et al.
Analysis and Deformulation of Polymeric Materials: Paints, Plastics, Adhesives, and Inks by Jan W. Gooch